The basic concept of this new edition remains unchanged: Emphasis is again put on a broader description of the general methods and processes for the synthesis, modification and characterization of macromolecules. These more fundamental chapters will be supplemented by 115 selected and detailed experiments. In addition to the preparative aspects the book also gives the reader an impression on the relation of chemical constitution and morphology of Polymers to their properties, as well as on their application areas. Thus, an additional textbook will not be needed in order to understand the experiments.